Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 2-Cyclopropylethyl methanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 반응물 | 2-Cyclopropylethan-1-ol | HCID 137642 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-Cyclopropylethyl methanesulfonate | HCID 14557809 | — |
반응 단계
A 0.5 g quantity of 2-cyclopropylethanol and 3.1 ml of triethylamine were dissolved in 10 ml of ethyl acetate, and 0.75 ml of methanesulfonyl chloride was added with ice-cooling and stirring. After stirring for 30 minutes, water was added to the reaction mixture and extraction was performed. The organic layer was washed with water twice and concentrated by removing the solvent under reduced pressure to give 1 g of pale yellow oily 2-cyclopropylethyl methanesulfonate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08637559B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-9027ce4a434f4a6d8f1ff10f40755bef |
| 출처 메모 | uspto-grants-2014_01 |