Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4,4'-Dihydroxybiphenyl → 4-Hydroxybenzoic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4,4'-Dihydroxybiphenyl | HCID 7112 | — |
| 반응물 | Dodecanedioic Acid | HCID 12736 | — |
| 생성물 | 4-Hydroxybenzoic Acid | HCID 135 | — |
반응 단계
Polymerization was carried out in the same way as Example 1, except that (A) preparing materials were changed to 4,4′-dihydroxybiphenyl, dodecanedioic acid, 4-hydroxybenzoic acid, acetic anhydride, and (B) a mixture of 4,4′-dihydroxybiphenyl, dodecanedioic acid, 4-hydroxybenzoic acid, acetic anhydride at a molar ratio of 1.05:1:2:4.1 in which 4,4′-dihydroxybiphenyl was excess by 5 mol % was prepared in a reactor vessel, thereby producing a thermoplastic resin in which 4-hydroxybenzoic acid was copolymerized with the resin of Example 1. A molecular structure, sealed end groups, and a sealing rate of ends are shown in Table 2, and changes in number average molecular mass and thermal conductivity before and after melting are shown in Table 3.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08637630B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-85734ecb7a8a4e57a35f03491fc78cc1 |
| 출처 메모 | uspto-grants-2014_01 |