Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Platinous chloride → HCID 178435846, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Platinous chloride | HCID 2770 | — |
| 반응물 | HCID 178435845 | HCID 178435845 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 178435846 | HCID 178435846 | — |
반응 단계
In a suitable 150 ml vessel 50 ml of dimethylformamide is brought to reflux and 20 mg 5-bromo octaethylporphine free base is added and dissolved. To this solution 8 mg platinum chloride is added and permitted to react for about 20 minutes. Thereafter, the reaction mixture is permitted to cool and crystal formation promoted by the addition of 50 ml distilled water. The reaction mixture is allowed to sit for about twenty four hours to increase crystal size. The reaction mixture is filtered by vacuum filtration and the solids retained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04885114 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-f01890c04f3b4fe4939f16b4f5a0396c |
| 출처 메모 | uspto-grants-1989_12 |