Sodium Carbonate → HCID 14234820, 화합물
반응식
Cl.[NH2:2][CH:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1.[CH2:16]([O:18][CH2:19][CH2:20]Br)[CH3:17].C(=O)([O-])[O-].[Na+].[Na+]>C(O)C>[CH2:16]([O:18][CH2:19][CH2:20][NH:2][CH:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1)[CH3:17]참가 물질
5
실험 절차
A mixture containing 7.8 g of the compound of Example 2, 6.7 g of 2-bromoethyl ethyl ether and 6.2 g of sodium carbonate in ethanol is brought to reflux with stirring for 20 hours.
후처리
- temperatureto reflux
출처 및 근거
- ORD 기록
- ord-4bcdb6f992fb4207a2c78dc5b16c6de6
- 출처 데이터셋
- uspto-grants-1989_12
- 특허 번호
- US04885373
반응 노트
불러오는 중…