13-Oxabicyclo[10.1.0]tridecane → Cyclododecanone
반응식
[O:1]1[CH:3]2[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH:2]12.[Cl-].[Li+]>>[C:2]1(=[O:1])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1참가 물질
3
반응 조건
- 온도
- 200 °C
실험 절차
25 g of epoxy-cyclododecane and 1 g of lithium chloride were dissolved in 20 g of N,N'-dimethyl ethylene urea and the solvent was stirred at 200° C. for 6 hours. The reaction mixture was analyzed to have a 94% yield of cyclododecanone.
출처 및 근거
- ORD 기록
- ord-7ae9b31cdbc147aa95cadb7d1820ee09
- 출처 데이터셋
- uspto-grants-1989_12
- 특허 번호
- US04885397
반응 노트
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