Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → HCID 19836535, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | p-Toluenesulfonic acid 1-methylheptyl ester | HCID 3912199 | — |
| 반응물 | 3'-Bromo-4'-hydroxy-4-acetylbiphenyl | HCID 14474361 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 19836535 | HCID 19836535 | — |
반응 단계
The above 3'-bromo-4'-hydroxy-4-acetylbiphenyl (200 g) was treated with 1.2 times equivalents of R 1-methylheptyl p-toluenesulfonate and potassium hydroxide in 97% ethanol (1 l) for 6 hours under reflux. The reaction mixture was worked up in a usual way to obtain crude oily 3'-bromo-4'-(1-methylheptyloxy)-4-acetylbiphenyl (163 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04886622 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-a1bd88eaf8ec4544ad9ec66057274992 |
| 출처 메모 | uspto-grants-1989_12 |