Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(5-Aminopentyl)diethylamine → P,P-bis(2,2-dimethyl-1-aziridinyl)-N-(5-diethylamino-1-pentyl)-phosphinic amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (5-Aminopentyl)diethylamine | HCID 4584949 | — |
| 반응물 | P,P-bis(2,2-dimethyl-1-aziridinyl)phosphinyl chloride | HCID 13511140 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | P,P-bis(2,2-dimethyl-1-aziridinyl)-N-(5-diethylamino-1-pentyl)-phosphinic amide | HCID 19836605 | 90% |
반응 단계
In a similar manner 0.025 moles of P,P-bis(2,2-dimethyl-1-aziridinyl)phosphinoyl chloride in about 170 mL of THF are treated by dropwise addition with 0.026 moles of 5-diethylaminopentylamine in 25 mL of THF, stirred for several hours at ambient temperature, filtered, concentrated by rotary evaporation and vacuum distilled to yield about 90% pure P,P-bis(2,2-dimethyl-1-aziridinyl)-N-(5-diethylamino-1-pentyl)-phosphinic amide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04886790 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-9aef35d6daf64598af0ba4a421975c18 |
| 출처 메모 | uspto-grants-1989_12 |