Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 2-Amino-1-phenoxy-propene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | 1-Phenoxy-2-propanone | HCID 69313 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-Amino-1-phenoxy-propene | HCID 70048860 | — |
반응 단계
0.2 mol of phenoxyacetone in 200 ml of tetrahydrofuran is saturated at reflux temperature with ammonia gas with the addition of 0.2 g of p-toluene sulphonic acid. The mixture is allowed to stand at room temperature for 24 hours and the solvent is then removed by evaporation in vacuo. The evaporation residue is employed crude in the reaction of Example 5B.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04886804 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-f9508f221bf3480cacb1d5f539bc49be |
| 출처 메모 | uspto-grants-1989_12 |