Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Gamma-Butyrolactone → HCID 14997826, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Gamma-Butyrolactone | HCID 7302 | — |
| 반응물 | Hexadecylamine | HCID 8926 | — |
| 촉매 | Zincchloride | HCID 3007855 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 14997826 | HCID 14997826 | 797.2% |
반응 단계
A mixture of 59.45 g of hexadecylamine, 10.60 g of gamma butyrolactone, 200 ml of toluene, and 20 mg of zinc chloride was refluxed under nitrogen for three days. Upon cooling, the reaction mixture formed a precipitate which was recrystallized twice from toluene to yield 321.5 g (78.12%) of N-hexadecyl-4-hydroxybutyramide, m.p. 89.5°-90°
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04888328 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-ace47e70aa9a437aa3253784f3fa093f |
| 출처 메모 | uspto-grants-1989_12 |