참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 6-Methyluracil | HCID 12283 | — |
| 반응물 | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 178429729 | HCID 178429729 | 136.5% |
반응 단계
6-Methyluracil (25.0 g) was suspended in 1 liter of distilled pyridine with stirring and heated at 50° C. into solution. Phosphorus pentasulfide (12.6 g) was then added, and the mixture was refluxed for 20 hours. The solution was concentrated under reduced pressure, then the residue was refluxed with 500 ml of ethanol for one hour. Insoluble materials were removed by filtration and the filtrate was concentrated under reduced pressure. The residue was recrystallized from ethanol, affording 5.5 g of the objective compound as colorless crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04888332 |
|---|
| 출처 데이터셋 | uspto-grants-1989_12 |
|---|
| ORD ID | ord-8803435dd1da4637b5700b006de1fda9 |
|---|
| 출처 메모 | uspto-grants-1989_12 |
|---|
