Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl chloroformate → 1-Ethoxycarbonyl-1-phenythiosemicarbazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl chloroformate | HCID 10928 | — |
| 반응물 | 1-Phenylthiosemicarbazide | HCID 2781094 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Ethoxycarbonyl-1-phenythiosemicarbazide | HCID 85773191 | — |
반응 단계
A mixture of 1-phenylthiosemicarbazide (25 g), ethanol (180 ml) and ethyl chloroformate (17 ml) was heated under reflux with stirring for 30 minutes. The mixture was cooled to room temperature and the solid was filtered, washed with ethanol and then with ether to give 28.9 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04889553 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-ec16df487b4344ac9ab14b8560048c96 |
| 출처 메모 | uspto-grants-1989_12 |