참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrazinecarboxaldehyde | HCID 12229 | — |
| 반응물 | Ethyl thiooxamate | HCID 2733398 | — |
| 생성물 | (N-Formylhydrazino)-imino acetic acid ethyl ester | HCID 86590617 | 76.3% |
반응 단계
A mixture of ethyl thioxamate (10.55 g, 79.2 mmol) and formylhydrazine (5.00 g, 83.2 mmol) was heated at 65° C. for 30 minutes and stirred in accordance with a method described in Collect. Czech Chem. Commun., 1984, 49, p2492. After cooling, the precipitated crystal was collected by filteration and washed with ethanol to give (N-formylhydrazino)-imino acetic acid ethyl ester (9.62 g). Yield: 76%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06645956B1 |
|---|
| 출처 데이터셋 | uspto-grants-2003_11 |
|---|
| ORD ID | ord-6e3b649091e04ec88be4164ed2ff41fb |
|---|
| 출처 메모 | uspto-grants-2003_11 |
|---|
