참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Methylimidazole | HCID 1390 | — |
| 반응물 | Butyl Chloride | HCID 8005 | — |
| 생성물 | HCID 178448538 | HCID 178448538 | 98.3% |
반응 단계
251.4 g of 1-chlorobutane (2.7 mol) are loaded into a 1 l glass reactor. The mixture is heated to 60° C., and then 148.6 g of 1-methylimidazole (1.8 mol) are poured in dropwise, with stirring. The mixture is left to react for 24 h at 80° C. The reaction mixture is evaporated under vacuum. 309 g of 1-butyl-3-methylimidazolium chloride are obtained in the form of a yellowish solid (yield=98%). The product is used as it is without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06700007B2 |
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| 출처 데이터셋 | uspto-grants-2004_03 |
|---|
| ORD ID | ord-68bc9c3131dd4c65bf273fb78a69005b |
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| 출처 메모 | uspto-grants-2004_03 |
|---|