4-Chloroaniline → (E)-styryl-N-4-chlorophenyl Sulfonamide

HRID 479716노트

반응식

HRID 479716 반응식
[CH:1](/[S:9](Cl)(=[O:11])=[O:10])=[CH:2]\[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[Cl:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][CH:15]=1>>[CH:1](/[S:9]([NH:18][C:17]1[CH:19]=[CH:20][C:14]([Cl:13])=[CH:15][CH:16]=1)(=[O:11])=[O:10])=[CH:2]\[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 78124-ChloroanilineHCID 5369377(E)-2-phenylethene-1-sulfonyl chloride

생성물 1

HCID 8497751(E)-styryl-N-4-chlorophenyl Sulfonamide수율 56%

실험 절차

A solution of (E)-styrylsulfonyl chloride (10 mmol) and 4-chloroaniline (10 mmol) was subjected to General Procedure 1, part B. The title compound, melting point 107-109° C. was obtained in 56% yield.

출처 및 근거

ORD 기록
ord-4d97edb1a41243d3902ee458ef565d4e
출처 데이터셋
uspto-grants-2003_11
특허 번호
US06646009B2

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