N-Methylaniline → HCID 9944278, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9](Cl)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[CH3:15][NH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9]([N:16]([CH3:15])[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)(=[O:11])=[O:10])=[CH:5][CH:4]=1

참가 물질

반응물 2

HCID 7515N-Methylaniline

HCID 12114473HCID 12114473, 화합물

생성물 1

HCID 9944278HCID 9944278, 화합물수율 80.9%

실험 절차

A solution of (E)-4-methoxystyrylsulfonyl chloride (10 mmol) and N-methyl aniline (10 mmol) was subjected to General Procedure 1, part B. The title compound, melting point 126-129° C., was obtained 80.9% yield.

출처 및 근거

ORD 기록: ord-f3cb0222c2424723aae33280aca55fd1
출처 데이터셋: uspto-grants-2003_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06646009B2

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