Sulfanilamide → HCID 10177070, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9](Cl)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[S:15]([NH2:25])(=[O:24])([C:17]1[CH:22]=[CH:21][C:20]([NH2:23])=[CH:19][CH:18]=1)=[O:16]>>[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9]([NH:23][C:20]2[CH:21]=[CH:22][C:17]([S:15](=[O:24])(=[O:16])[NH2:25])=[CH:18][CH:19]=2)(=[O:11])=[O:10])=[CH:5][CH:4]=1

참가 물질

반응물 2

HCID 5333Sulfanilamide

HCID 12114473HCID 12114473, 화합물

생성물 1

HCID 10177070HCID 10177070, 화합물수율 46.2%

실험 절차

A solution of (E)-4-methoxystyrylsulfonyl chloride (10 mmol) and sulfanilamide (10 mmol) was subjected to General Procedure 1, part B. The title compound, melting point 181-183° C., was obtained in 46.2% yield.

출처 및 근거

ORD 기록: ord-cb6bd9ad431d47ca9ba06de9f570df6e
출처 데이터셋: uspto-grants-2003_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06646009B2

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