참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dione | HCID 70423 | — |
| 반응물 | HCID 178427422 | HCID 178427422 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Quinacridone | HCID 13976 | — |
반응 단계
20 g of C.I. pigment red 122 having an average primary particle diameter of 90 nm (in which the content of metal ions having a valence of at least 2 was 450 ppm), 4 g of a commercially available dye C.I. acid red 249 and 110 g of deionized water were mixed, aqueous ammonia was added so as to adjust the pH of a mixture liquid to 9.0, and the mixture liquid was dispersed with a paint shaker in the presence of zirconia beads as media for approximately 5 hours, to obtain a water-based pigment dispersion. The obtained water-based pigment dispersion had a high viscosity and caused flocculation. Further, the water-based pigment dispersion was diluted so as to have a concentration of 3% by weight, and the diluted water-based pigment dispersion was dropped on No.2 filter paper, to show bleeding of the dye.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06648954B2 |
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| 출처 데이터셋 | uspto-grants-2003_11 |
|---|
| ORD ID | ord-a93018f0c5a346c381a6a0cd5b462802 |
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| 출처 메모 | uspto-grants-2003_11 |
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