Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-Diethyl-1,3-propanediamine → 5-Nitroisophthalic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-Diethyl-1,3-propanediamine | HCID 61011 | — |
| 반응물 | Dimethyl 5-nitroisophthalate | HCID 83316 | — |
| 생성물 | 5-Nitroisophthalic acid | HCID 12069 | — |
| 생성물 | 3-Diethylaminopropylamide | HCID 86585225 | — |
반응 단계
Fifty parts of dimethyl 5-nitroisophthalate and 130 parts of N,N-diethyl-1,3-propanediamine were reacted for about four hours at 80 to 100° C. under a slight vacuum. After confirming the disappearance of the starting material dimethyl 5-nitroisophthalate and monoamide compounds, the excess N,N-diethyl-1,3-propanediamine was removed under vacuum, yielding 92 parts of 5-nitroisophthalic acid bis-3-diethylaminopropylamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06653000B2 |
| 출처 데이터셋 | uspto-grants-2003_11 |
| ORD ID | ord-88c9270eb2f04da9be0c30f71a9ca05e |
| 출처 메모 | uspto-grants-2003_11 |