Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,6-Cleve's acid → HCID 12094653, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,6-Cleve's acid | HCID 8408 | — |
| 반응물 | 5-Nitroisophthaloyl chloride | HCID 83451 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | HCID 12094653 | HCID 12094653 | — |
반응 단계
22.33 g (0.10 mol) of 5-amino-2-naphthalenesulfonic acid was suspended in 150 mL of pyridine and added to the above di-acid chloride in 50 mL (50:50) of dioxane and CHCl3 under vigorous stirring for 1-2 hrs. The crude product was precipitated with dioxane. The oily product was collected on a Büchner funnel. The brown colored oily product was dissolved in 500 mL water, then allowed to precipitate out over 30 min. The solid material was collected using filtration. It yielded 16.2 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06653321B1 |
| 출처 데이터셋 | uspto-grants-2003_11 |
| ORD ID | ord-5e3368348bc7428f8858fabd35c3d318 |
| 출처 메모 | uspto-grants-2003_11 |