Cyclopentylacetic acid → N-(cyclopentylacetyl)-L-alanine

HRID 480723

반응식

HRID 480723 반응식
[CH:1]1([CH2:6][C:7]([OH:9])=O)[CH2:5][CH2:4][CH2:3][CH2:2]1.Cl.C[O:12][C:13](=[O:17])[C@H:14]([CH3:16])[NH2:15]>>[CH:1]1([CH2:6][C:7]([NH:15][C@H:14]([C:13]([OH:17])=[O:12])[CH3:16])=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5]1

참가 물질

3

반응물 2

HCID 71606Cyclopentylacetic acidHCID 2733257Alanine methyl ester hydrochloride

생성물 1

HCID 29895597N-(cyclopentylacetyl)-L-alanine

실험 절차

Following General Procedure A above using cyclopentylacetic acid (Aldrich) and L-alanine methyl ester hydrochloride (Sigma), the title compound was prepared as a solid having a melting point of 4346° C. Purification was by recrystallization from ethyl acetate/hexanes.

후처리

  1. customPurification
  2. customwas by recrystallization from ethyl acetate/hexanes

출처 및 근거

ORD 기록
ord-ae8d3d5148d34bc09c7f0315a756b70d
출처 데이터셋
uspto-grants-2003_11
특허 번호
US06653303B1

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