반응식
C([O:3][C:4]([C:6]1[CH:11]=[CH:10][C:9]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][C:25]([F:37])([F:36])[C:26]([F:35])([F:34])[C:27]([F:33])([F:32])[C:28]([F:31])([F:30])[F:29])=[C:14]([F:38])[C:13]=2[F:39])=[CH:8][CH:7]=1)=[O:5])C.FC1C(F)=C(OCCCCC(F)(F)C(F)(F)C(F)(F)C(F)(F)F)C=CC=1C1C=CC(C(O)=O)=CC=1>>[F:39][C:13]1[C:14]([F:38])=[C:15]([O:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][C:25]([F:36])([F:37])[C:26]([F:34])([F:35])[C:27]([F:32])([F:33])[C:28]([F:31])([F:29])[F:30])[CH:16]=[CH:17][C:12]=1[C:9]1[CH:10]=[CH:11][C:6]([C:4]([OH:5])=[O:3])=[CH:7][CH:8]=1참가 물질
3
반응물 2
생성물 1
실험 절차
2′,3′-Difluoro-4′-(7,7,8,8,9,9,10,10,10-nonafluoro-decyloxy)-biphenyl-4-carboxylic acid (14B) was prepared from 2′,3′-difluoro-4′-(7,7,8,8,9,9,10,10,10-nonafluoro-decyloxy)-biphenyl-4-carboxylic acid ethyl ester (13B) as described in the preparation 2′,3′-difluoro-4′-(5,5,6,6,7,7,8,8,8-nonafluoro-octyloxy)-biphenyl-4-carboxylic acid (14 A) yielding 2′,3′-difluoro-4′-(7,7,8,8,9,9,10,10,10-nonafluoro-decyloxy)-biphenyl-4-carboxylic acid (14B) as a white solid (88%).
출처 및 근거
- ORD 기록
- ord-48eda4666b73409dad8f24bb0925bcc3
- 출처 데이터셋
- uspto-grants-2004_03
- 특허 번호
- US06703082B1
연결된 노트
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