Carbamic acid, ethyl ester → Methyl (3-{[(methoxycarbonyl)amino]methyl}-3,5,5-trimethylcyclohexyl)carbamate

HRID 481800

반응식

HRID 481800 반응식
[NH2:1][C:2]([O:4][CH2:5]C)=[O:3].[CH3:7][C:8]1([CH3:18])[CH2:13][C:12]([CH2:15][NH2:16])([CH3:14])[CH2:11][CH:10](N)[CH2:9]1>>[CH3:5][O:4][C:2]([NH:16][CH2:15][C:12]1([CH3:14])[CH2:13][C:8]([CH3:18])([CH3:7])[CH2:9][CH:10]([NH:1][C:2]([O:4][CH3:5])=[O:3])[CH2:11]1)=[O:3]

참가 물질

3

반응물 2

HCID 5641Carbamic acid, ethyl esterHCID 17857Isophorone diamine

생성물 1

HCID 3246761Methyl (3-{[(methoxycarbonyl)amino]methyl}-3,5,5-trimethylcyclohexyl)carbamate수율 98.1%

실험 절차

The thus-prepared crude reaction solution was analyzed by gas chromatography and it was confirmed that a urethane compound corresponding to IPDA, that is, 3-methoxycarbonylaminomethyl-3,5,5-trimethyl-1-methoxycarbonylaminocyclohexane, was produced in a yield of 98.1% based on IPDA.

후처리

  1. customThe thus-prepared crude
  2. customreaction solution

출처 및 근거

ORD 기록
ord-440f133152284332aec5f199f2f00935
출처 데이터셋
uspto-grants-1998_08
특허 번호
US05789614

연결된 노트

불러오는 중…