Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → N-Benzyl-2-chloro-9-isopropyl-9H-purin-6-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | 2,6-dichloro-9-(propan-2-yl)-9H-purine | HCID 11218490 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | N-Benzyl-2-chloro-9-isopropyl-9H-purin-6-amine | HCID 10733091 | 85% |
반응 단계
2,6-dichloro-9-isopropylpurine (1 mmol) and benzylamine (3.5 mmol) were heated with stirring in 3 ml of n-butanol (3 hour, 110° C.). The reaction mixture (after evaporation of n-butanol) was worked up as above for the compound 2, yield 85-90%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06703395B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-d2bcde2ca2704df1811ca52f0c53f035 |
| 출처 메모 | uspto-grants-2004_03 |