Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole → HCID 178488922, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole | HCID 178488923 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178488922 | HCID 178488922 | 102.4% |
반응 단계
2-(4-Methoxyphenyl)-4-(2-nitrophenyl)imidazole (10 g) is mixed with EtOH (80 ml) and 5% Pd-C (wet, 2 g). The mixture is shaken under hydrogen at 50 psi for 45 min. then filtered through Celite. The filtrate is evaporated under reduced pressure to yield 2-(4-methoxyphenyl)-4-(2-aminophenyl)imidazole (9.2 g) as a brown solid which is used in the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05792766 |
| 출처 데이터셋 | uspto-grants-1998_08 |
| ORD ID | ord-98cf92f716584d32a3b44bbdbb725d0f |
| 출처 메모 | uspto-grants-1998_08 |