참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ammonium nitrate | HCID 22985 | — |
| 반응물 | Bentazone-sodium | HCID 13124860 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Bentazone ammonium | HCID 131720800 | 73.2% |
반응 단계
8 g of ammonium nitrate were introduced at 50° C. with stirring into a solution of 26.3 g of bentazone-sodium in 21.7 g of water, and the reaction mixture was subsequently stirred for a further hour. After cooling to 20° C., the precipitate was filtered off, washed twice with 5 ml of ice water in each case and dried under reduced pressure and at 50° C. 18.9 g of bentazone-ammonium of 99% purity were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US05795983 |
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| 출처 데이터셋 | uspto-grants-1998_08 |
|---|
| ORD ID | ord-7473581cb0484df3816afca8d4efcaec |
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| 출처 메모 | uspto-grants-1998_08 |
|---|