Methane → HCID 12968235, 화합물

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[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:9][C:10]3[CH:32]=[C:31]([OH:33])[CH:30]=[CH:29][C:11]=3[C:12]=2[CH:13]([C:15]2[CH:20]=[CH:19][C:18]([O:21][CH2:22][CH2:23][N:24]3[CH2:28][CH2:27][CH2:26][CH2:25]3)=[CH:17][CH:16]=2)O)=[CH:4][CH:3]=1.C>>[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:9][C:10]3[CH:32]=[C:31]([OH:33])[CH:30]=[CH:29][C:11]=3[C:12]=2[CH2:13][C:15]2[CH:16]=[CH:17][C:18]([O:21][CH2:22][CH2:23][N:24]3[CH2:28][CH2:27][CH2:26][CH2:25]3)=[CH:19][CH:20]=2)=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 297Methane

HCID 12968234[2-(4-Hydroxyphenyl)-6-hydroxybenzofuran-3-yl][4-[2-(1-pyrrolidinyl)ethoxy]phenyl]methanol

생성물 1

HCID 12968235HCID 12968235, 화합물수율 52.4%

실험 절차

550 mg (1.2 mmol) of the product of Example 11 was reduced to the methane by the method described in Example 2. This yielded 270 mg of the title compound as an amorphous powder.

출처 및 근거

ORD 기록: ord-bd7aa0b2cd034660b2ef6082c537ae47
출처 데이터셋: uspto-grants-2004_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06703407B1

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