Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Isocyanate → N,2-Dimethyl-2,3-dihydro-1H-indole-1-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Isocyanate | HCID 12228 | — |
| 반응물 | 2-Methylindoline | HCID 23305 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N,2-Dimethyl-2,3-dihydro-1H-indole-1-carboxamide | HCID 12321965 | 89% |
반응 단계
1 mole of 2-methylindoline is dissolved in 300 ml of toluene and 1 mole of methyl isocyanate is added, the temperature not rising above 25° C. The mixture is left to stand for 1 day and the resulting precipitate is then filtered off. N-Methylaminocarbonyl-2-methylindoline with a melting point of 158°-160° C. is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04574124 |
| 출처 데이터셋 | uspto-grants-1986_03 |
| ORD ID | ord-67cd72da9e004d86b4df692275ac9af9 |
| 출처 메모 | uspto-grants-1986_03 |