4,5-Dihydro-2-(methylthio)thiazole → HCID 70454469, 화합물

HRID 482683

반응식

HRID 482683 반응식
CS[C:3]1[S:4][CH2:5][CH2:6][N:7]=1.Cl.[Cl:9][C:10]1[C:11]([NH:17][NH2:18])=[C:12]([CH3:16])[CH:13]=[CH:14][CH:15]=1>C(O)(C)C>[Cl:9][C:10]1[C:11]([NH:17][NH:18][C:3]2[S:4][CH2:5][CH2:6][N:7]=2)=[C:12]([CH3:16])[CH:13]=[CH:14][CH:15]=1

참가 물질

4

반응물 2

HCID 883244,5-Dihydro-2-(methylthio)thiazoleHCID 2800160(2-Chloro-6-methylphenyl)hydrazine hydrochloride

생성물 1

HCID 70454469HCID 70454469, 화합물

시약·촉매·용매 1

HCID 3776Isopropanol용매2회

실험 절차

A solution of 11.2 g (5% excess) of 2-methylthio-2-thiazoline in 20 ml of isopropanol was added slowly in the course of 30 minutes to a suspension, which was stirred under reflux, of 15.5 g (0.08 mol) of 3-chloro-2-tolyl-hydrazine hydrochloride in 100 ml of isopropanol.

출처 및 근거

ORD 기록
ord-2ca251c893084a03b38c979895c8ff64
출처 데이터셋
uspto-grants-1986_03
특허 번호
US04575501

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