1-Naphthaldehyde → 1,3-Dithiolane, 2-(1-naphthalenyl)-

HRID 482783노트

반응식

[C:1]1([CH:11]=O)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[CH2:13]([SH:16])[CH2:14][SH:15]>>[C:1]1([CH:11]2[S:16][CH2:13][CH2:14][S:15]2)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1

참가 물질

반응물 2

HCID 61951-Naphthaldehyde

HCID 109021,2-Ethanedithiol

생성물 1

HCID 108681811,3-Dithiolane, 2-(1-naphthalenyl)-수율 96%

실험 절차

Following the general procedure as in Example 1, 38.27 gm (0.245 moles) of α-naphthaldehyde and 23.58 gm (0.25 moles) of 1,2-ethanedithiol gave, after evacuating the volatiles, 54.56 gm (0.235 moles) of an orange colored oil (96% yield).

후처리

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출처 및 근거

ORD 기록: ord-1513683aee744ec188753c0c2f23074d
출처 데이터셋: uspto-grants-1986_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04575565

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