Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 178487721, 화합물 → HCID 178487715, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 178487721 | HCID 178487721 | — |
| 용매 | 1,1'-Biphenyl, mixt. with 1,1'-oxybis(benzene) | HCID 24670 | — |
| 생성물 | HCID 178487715 | HCID 178487715 | 97% |
반응 단계
A suspension of 4-hydroxy-7-methoxyquinoline-3-carboxylic acid (4.0 g) in Dowtherm A (75 mL) was heated at reflux for 2 hrs. The resulting brown solution was allowed to slowly cool to ambient temperature. The resulting precipitate was isolated by filtration and then dried in a vacuum oven at 80° C. for 2.5 days to provide 3.1 g of 7-methoxyquinolin-4-ol as a light tan solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06703402B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-0f2302e84a904c439d868abfbb7436ce |
| 출처 메모 | uspto-grants-2004_03 |