Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylenediamine → (9-Chloro-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylenediamine | HCID 3301 | — |
| 반응물 | N-Methylethylenediamine | HCID 8014 | — |
| 반응물 | 3-Chloro-2-fluorobenzoic acid | HCID 302931 | — |
| 반응물 | (1-Methyl-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester | HCID 72957243 | — |
| 생성물 | (9-Chloro-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester | HCID 86585810 | — |
반응 단계
(9-chloro-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester was prepared in an analogous fashion to (1-methyl-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester, prepared in Example 1, by replacing 2-fluorobenzoic acid with 2-fluoro-3-chlorobenzoic acid and N-methylethylenediamine with ethylenediamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06703387B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-156eba81e47e464d806a53a6449d9179 |
| 출처 메모 | uspto-grants-2004_03 |