Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Sulfoxide → 2-trifluoromethylphenyl-S,S-dimethylsulfilimine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Sulfoxide | HCID 679 | — |
| 반응물 | 2-Nitro-alpha,alpha,alpha-trifluorotoluene | HCID 9795 | — |
| 반응물 | 2-(Trifluoromethyl)phenyl isocyanate | HCID 16794 | — |
| 생성물 | 2-trifluoromethylphenyl-S,S-dimethylsulfilimine | HCID 13391192 | — |
반응 단계
The process of claim 18 in which 2-trifluoromethylnitrobenzene is carbonylated to 2-trifluoromethylphenyl isocyanate, which is reacted with dimethylsulfoxide to obtain N-(2-trifluoromethylphenyl)-S,S-dimethylsulfilimine, rearranged to a 2-(methylthiomethyl)-6-trifluoromethylaniline, and desulfurized to 2-methyl-6-trifluoromethyl aniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04578514 |
| 출처 데이터셋 | uspto-grants-1986_03 |
| ORD ID | ord-564a0531b1c74f918c075c91dda58357 |
| 출처 메모 | uspto-grants-1986_03 |