Thionyl Chloride → 2-(Octyloxy)benzoyl chloride

반응식

[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12](O)=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:21])=O>>[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12]([Cl:21])=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 200827752-(Octyloxy)benzoic acid

생성물 1

HCID 203111572-(Octyloxy)benzoyl chloride

실험 절차

First, octyloxybenzoic acid was heated in thionyl chloride under reflux until complete dissolution. Excess thionyl chloride was removed by vacuum distillation. Thus there was obtained octyloxybenzoic acid chloride.

후처리

temperatureunder reflux until complete dissolution
customExcess thionyl chloride was removed by vacuum distillation

출처 및 근거

ORD 기록: ord-65b436956dee4667b9a4e64adcfcd867
출처 데이터셋: uspto-grants-1993_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05225105

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