Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 10466579, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 4-Nitro-3-phenyl-L-alanine | HCID 13706 | — |
| 반응물 | Potassium cyanate | HCID 11378442 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 10466579 | HCID 10466579 | 82% |
반응 단계
A solution of p-nitrophenylalanine (4.2 g, Fluka) and potassium cyanate (1.62 g) in water (6 ml) was refluxed for 1 hour. C.HCl (3 ml) was added and the mixture refluxed for a further 10 minutes, then cooled, diluted with water and filtered. The residue was washed with water and dried to give the desired product as a straw-coloured solid (3.85 g). The 200 MHz 1H NMR was consistent with the proposed structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05225431 |
| 출처 데이터셋 | uspto-grants-1993_07 |
| ORD ID | ord-62efc28f41c543b7913ba1e431fd9ca5 |
| 출처 메모 | uspto-grants-1993_07 |