Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → Benzoyl chloride, 4-(tetradecyloxy)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 4-(Tetradecyloxy)benzoic acid | HCID 289410 | — |
| 촉매 | Chloroform | HCID 6212 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Benzoyl chloride, 4-(tetradecyloxy)- | HCID 9998158 | 102.4% |
반응 단계
A mixture of 50 g of p-(tetradecyloxy)benzoic acid and 28.46 g of oxalyl chloride in 500 ml of chloroform containing 10 drops of N,N-dimethylformamide is stirred for 18 hours at ambient temperature. The solvent is evaporated and the residue dissolved in ether, filtered and evaporated to give 54 g of the desired product as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05225425 |
| 출처 데이터셋 | uspto-grants-1993_07 |
| ORD ID | ord-1525193c99d5448682c4d78a085ff665 |
| 출처 메모 | uspto-grants-1993_07 |