참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dichlorodifluoromethane | HCID 6391 | — |
| 반응물 | 1-Bromo-1,2,2-trifluoroethene | HCID 11730 | — |
| 반응물 | Bis(fluoroxy)perfluoromethane | HCID 140054 | — |
| 용매 | Nitrogen | HCID 947 | — |
| 생성물 | 4-Bromo-2,2,4,5,5-pentafluoro-1,3-dioxolane | HCID 19745410 | — |
반응 단계
Into a multineck glass reactor equipped with: magnetic entrainment mechanical stirrer, reflux cooler, thermocouple, inner plunging pipes for introducing the reagents, and maintained at a temperature of -70° C., there were simultaneously fed--after having introduced 75 ml of dichlorodifluoromethane--0.75 l of bis(fluoroxy)difluoromethane at a flowrate of 0.375 l/h diluted with N2 (0.5 l/h) and bromotrifluoroethylene (5.4 g/h) for 2 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05225576 |
|---|
| 출처 데이터셋 | uspto-grants-1993_07 |
|---|
| ORD ID | ord-6836a1b108ea495ebd618e95c9b17ff5 |
|---|
| 출처 메모 | uspto-grants-1993_07 |
|---|
