Thionyl Chloride → HCID 53411290, 화합물

HRID 483941노트

반응식

HRID 483941 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7](O)=[O:8].S(Cl)([Cl:15])=O>C1C=CC=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7]([Cl:15])=[O:8]

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 746313-(3-Chlorophenyl)prop-2-enoic acid

생성물 1

HCID 53411290HCID 53411290, 화합물

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

100 ml of benzene was added to 18.3 grams of m-chlorocinnamic acid. 12 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 80° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.

후처리

  1. customat ambient temperature
  2. customwas elevated to 80° C.
  3. distillationBenzene and thionyl chloride were distilled off
  4. customthe residue was dried thoroughly under reduced pressure

출처 및 근거

ORD 기록
ord-05381250536a4912991c8429137f6a18
출처 데이터셋
uspto-grants-1993_07
특허 번호
US05229002

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