Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dimethyl-4-nitroaniline → 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dimethyl-4-nitroaniline | HCID 28159 | — |
| 반응물 | 2-Chloro-1-pyrroline | HCID 13520141 | — |
| 생성물 | 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline | HCID 20272394 | — |
반응 단계
A mixture of 2-chloro-1-pyrroline, prepared as in Example 1, and 19.9 g (0.12 mole) of the aniline product of Example 6 were heated at reflux overnight, according to the general method of Example 8. The title compound was isolated and used for subsequent reactions without further purification. Structure assignment was supported by nmr and infrared spectra.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04533739 |
| 출처 데이터셋 | uspto-grants-1985_08 |
| ORD ID | ord-b73808b27f264206b52ae5c5d7b1945f |
| 출처 메모 | uspto-grants-1985_08 |