Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Iodide → N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Iodide | HCID 4875 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide | HCID 12769237 | — |
| 반응물 | N,N-diallyl alpha-bromopropionamide | HCID 13036601 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide | HCID 13503503 | — |
반응 단계
The reaction mixture was washed with water and dried and the solvent was distilled off to obtain 3.8 g. of N,N-diallyl α-bromopropionamide. The product was admixed with 3.5 g. of N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide, 2.2 g. of potassium carbonate, 1.8 g. of potassium iodide and 50 ml. of acetone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04536209 |
| 출처 데이터셋 | uspto-grants-1985_08 |
| ORD ID | ord-bf2d6795dd0b49899e460acfaecd3e6b |
| 출처 메모 | uspto-grants-1985_08 |