Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Toluenesulfonyl chloride → HCID 13957272, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| 반응물 | 1-Octanol, 8-chloro- | HCID 90012 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 13957272 | HCID 13957272 | — |
반응 단계
p-Toluenesulphonyl chloride (20.5 g) was added to a mixture of 8-chloro-1-octanol (17.7 g) and pyridine (50 ml) of 0°. After a hour the solution was added to ice and the mixture was extracted with ether. The ethereal solution was washed with dilute hydrochloric acid, dried with magnesium sulfate, and evaporated to yield the title compound as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04536503 |
| 출처 데이터셋 | uspto-grants-1985_08 |
| ORD ID | ord-b240b72b7cec4533bb47620064d06262 |
| 출처 메모 | uspto-grants-1985_08 |