4-Toluenesulfonyl chloride → HCID 13957272, 화합물

HRID 485299

반응식

HRID 485299 반응식
[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[Cl:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][OH:21]>N1C=CC=CC=1>[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7]([O:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][Cl:12])(=[O:9])=[O:8])=[CH:3][CH:2]=1

참가 물질

4

반응물 2

HCID 73974-Toluenesulfonyl chlorideHCID 900121-Octanol, 8-chloro-

생성물 1

HCID 13957272HCID 13957272, 화합물

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

p-Toluenesulphonyl chloride (20.5 g) was added to a mixture of 8-chloro-1-octanol (17.7 g) and pyridine (50 ml) of 0°. After a hour the solution was added to ice and the mixture was extracted with ether. The ethereal solution was washed with dilute hydrochloric acid, dried with magnesium sulfate, and evaporated to yield the title compound as an oil.

후처리

  1. additionAfter a hour the solution was added to ice
  2. extractionthe mixture was extracted with ether
  3. washThe ethereal solution was washed with dilute hydrochloric acid
  4. dry with materialdried with magnesium sulfate
  5. customevaporated

출처 및 근거

ORD 기록
ord-b240b72b7cec4533bb47620064d06262
출처 데이터셋
uspto-grants-1985_08
특허 번호
US04536503

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