Indazolinone → HCID 178456741, 화합물

HRID 485744

반응식

HRID 485744 반응식
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([OH:10])=[N:2]1.[CH:11]([N:14]1C(=O)O[C:17](=[O:18])[C:16]2=[CH:22][CH:23]=[CH:24][CH:25]=[C:15]12)([CH3:13])[CH3:12]>>[CH:11]([NH:14][C:15]1[CH:25]=[CH:24][CH:23]=[CH:22][C:16]=1[C:17]([N:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([OH:10])=[N:2]1)=[O:18])([CH3:13])[CH3:12]

참가 물질

3

반응물 2

HCID 81829IndazolinoneHCID 39125701-(Propan-2-yl)-2H-3,1-benzoxazine-2,4(1H)-dione

생성물 1

HCID 178456741HCID 178456741, 화합물수율 71.3%

실험 절차

1H-Indazol-3-ol was reacted with N-isopropylisatoic anhydride according to the general procedure A above and afforded the desired amine as a yellow solid in 71.3% yield; m.p. 190°-192° C.

출처 및 근거

ORD 기록
ord-edb11c39280b447e934e311f8d912d60
출처 데이터셋
uspto-grants-1985_08
특허 번호
US04537966

연결된 노트

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