Indazolinone → HCID 178425486, 화합물

HRID 485748

반응식

HRID 485748 반응식
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([OH:10])=[N:2]1.[CH3:11][C:12]1[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][C:13]=1[N:19]1C(=O)O[C:22](=[O:23])[C:21]2=[CH:27][CH:28]=[CH:29][CH:30]=[C:20]12>>[CH3:11][C:12]1[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][C:13]=1[NH:19][C:20]1[CH:30]=[CH:29][CH:28]=[CH:27][C:21]=1[C:22]([N:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([OH:10])=[N:2]1)=[O:23]

참가 물질

3

반응물 2

HCID 81829IndazolinoneHCID 54162132N-(2,3-dimethylphenyl)isatoic anhydride

생성물 1

HCID 178425486HCID 178425486, 화합물수율 42.5%

실험 절차

1H-Indazol-3-ol was reacted with N-(2,3-dimethylphenyl)isatoic anhydride according to the general procedure A above and afforded the desired amine as a yellow solid in 42.5% yield; m.p. 182°-184° C.

출처 및 근거

ORD 기록
ord-00b06162e8eb416aa8c4501848ef8b2f
출처 데이터셋
uspto-grants-1985_08
특허 번호
US04537966

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