HCID 178445573, 화합물 → HCID 178447704, 화합물

반응식

[NH2:1][C:2]1[N:6]=[C:5]([S:7][CH2:8][CH2:9][CH2:10][S:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[NH:4][N:3]=1.C(SCCSCCSC1N=C2N(N=1)[C:36]([OH:39])=[CH:35][C:34]([CH3:40])=N2)CCCCC>>[CH2:12]([S:11][CH2:10][CH2:9][CH2:8][S:7][C:5]1[N:6]=[C:2]2[N:3]([N:4]=1)[C:36]([OH:39])=[CH:35][C:34]([CH3:40])=[N:1]2)[CH2:13][CH2:14][CH2:15][CH3:16]

참가 물질

반응물 2

HCID 178445573HCID 178445573, 화합물

HCID 1784477053-Amino-5-[3-(pentylthio)propylthio]-1,2,4-triazole

생성물 1

HCID 178447704HCID 178447704, 화합물

실험 절차

Compound 18 was prepared from Compound 9, using a procedure analogous to that described previously for Compound 20. The crude product was recrystallized from ethyl acetate to give a 24% yield of white solid, m.p. 121°-123° C. Analysis: Calculated for C14H22N4OS2 : C, 51.50; H, 6.79; N, 17.16. Found: C, 51.30; H, 6.69; N, 16.97.

후처리

customThe crude product was recrystallized from ethyl acetate

출처 및 근거

ORD 기록: ord-60e55e029af2488fbfd9b0ec64286d43
출처 데이터셋: uspto-grants-1994_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05292627

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