4-Cyanobenzaldehyde → HCID 19096399, 화합물

HRID 486710노트

반응식

HRID 486710 반응식
[C:1]([C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1)#[N:2].[CH:11]1([C:14](=[O:21])[CH2:15][C:16]([CH:18]2[CH2:20][CH2:19]2)=[O:17])[CH2:13][CH2:12]1>>[C:1]([C:3]1[CH:10]=[CH:9][C:6]([CH:7]=[C:15]([C:14]([CH:11]2[CH2:13][CH2:12]2)=[O:21])[C:16]([CH:18]2[CH2:20][CH2:19]2)=[O:17])=[CH:5][CH:4]=1)#[N:2]

참가 물질

3

반응물 2

HCID 660424-CyanobenzaldehydeHCID 137807821,3-Dicyclopropylpropane-1,3-dione

생성물 1

HCID 19096399HCID 19096399, 화합물

실험 절차

The procedure described in Example 19 was repeated by using 3.78 g 4-cyanobenzaldehyde and 2.23 g 1,3-dicyclopropyl-1,3-propanedione. Yield 1.5 9, mp 100°-102° C.

후처리

  1. customYield 1.5 9, mp 100°-102° C.

출처 및 근거

ORD 기록
ord-b6ed3ea583d14a5bbbcd0ffd92a159c1
출처 데이터셋
uspto-grants-1994_03
특허 번호
US05292771

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