2-Bromohexanoic acid → 6-Bromohexanoyl chloride

HRID 487038

반응식

HRID 487038 반응식
[Br:1][CH:2]([CH2:6][CH2:7][CH2:8]C)C(O)=O.[C:10](Cl)(=O)[C:11]([Cl:13])=[O:12]>CN(C)C=O>[Br:1][CH2:2][CH2:6][CH2:7][CH2:8][CH2:10][C:11]([Cl:13])=[O:12]

참가 물질

4

반응물 2

HCID 120132-Bromohexanoic acidHCID 65578Oxalyl chloride

생성물 1

HCID 898486-Bromohexanoyl chloride

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

58.5 g of (0.3 moles) of 6 bromohexanoic acid and 85 ml of oxalyl chloride are placed in a 250-ml flask with a magnetic agitator. The mixture is agitated and 1 milliliter of dimethylformamide (DMF) is added.

출처 및 근거

ORD 기록
ord-b0c2c43ef3fd413fb7975f6bb0c6f238
출처 데이터셋
uspto-grants-1994_03
특허 번호
US05294463

연결된 노트

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