Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trichloromethylsilane → HCID 131718361, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trichloromethylsilane | HCID 6399 | — |
| 반응물 | Neophyl chloride | HCID 68191 | — |
| 반응물 | Magnesium | HCID 5462224 | — |
| 반응물 | HCID 178418740 | HCID 178418740 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 131718361 | HCID 131718361 | 65% |
반응 단계
In accord with the procedure of Example 1, neophylmagnesium chloride was prepared from 674 g (4 mol) of neophyl chloride and 105 g (4.4 mol) of magnesium turnings in 1.5 liters of dry THF. The neophylmagnesium chloride was added to 598 g (4 mol) of methyltrichlorosilane and 2 g of cuprous cyanide in 500 ml of THF. 640 g (65% of theory) of neophylmethyldichlorosilane was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05296624 |
| 출처 데이터셋 | uspto-grants-1994_03 |
| ORD ID | ord-c8ea5e0ccad847beb6efceb6b6122ccd |
| 출처 메모 | uspto-grants-1994_03 |