Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Chloro-1,2-phenylene)dimethanol → 1,2-Benzenedimethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Chloro-1,2-phenylene)dimethanol | HCID 10899147 | — |
| 반응물 | 2-Methyl-4-chloro-1,3-butanediol | HCID 19091713 | — |
| 생성물 | 1,2-Benzenedimethanol | HCID 69153 | — |
| 생성물 | 4-Chlorobutane-1,3-diol | HCID 5152901 | — |
반응 단계
Example 1 was repeated except for using 10.53 g (76 mmoles) of 2-methyl-4-chloro-1,3-butanediol and 6.00 g (35 mmoles) of 4-chloro-o-xylylene glycol, instead of 9.48 g (76 mmoles of 4-chloro-1,3-butanediol and 4.76 g (35 mmoles) of o-xylylene glycol, respectively, to obtain spiro[7-chloro-1,5-dihydro-2,4-benzodioxepin-4'-methylene-5'-methyl-3,2'-[1,3dioxane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05298631 |
| 출처 데이터셋 | uspto-grants-1994_03 |
| ORD ID | ord-ae2e8084b83e42abbde00fff1507fa06 |
| 출처 메모 | uspto-grants-1994_03 |