Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Chloro-1,2-phenylene)dimethanol → 1,2-Benzenedimethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Chloro-1,2-phenylene)dimethanol | HCID 10899147 | — |
| 반응물 | 3-Methyl-5-chloro-1,4-pentanediol | HCID 19091716 | — |
| 생성물 | 1,2-Benzenedimethanol | HCID 69153 | — |
| 생성물 | 5-Chloro-1,4-pentanediol | HCID 19091715 | — |
반응 단계
Example 8 was repeated except for using 20.9 g (137 mmoles) of 3-methyl-5-chloro-1,4-pentanediol and 4.94 g (28.6 mmoles) of 4-chloro-o-xylylene glycol, instead of 19.0 g (137 mmoles) of 5-chloro-1,4-pentanediol and 3.95 g (28.6 mmoles) of o-xylylene glycol, respectively, to obtain spiro[7-chloro-1,5-dihydro-2,4-benzodioxepin-4'-methylene-5'-methyl-3,2'-[1,3]dioxepane].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05298631 |
| 출처 데이터셋 | uspto-grants-1994_03 |
| ORD ID | ord-dbb789fdbf02448bb80bd265e0933b4e |
| 출처 메모 | uspto-grants-1994_03 |