Potassium Carbonate → HCID 178472280, 화합물

HRID 488182

반응식

HRID 488182 반응식
[CH2:1]([O:3][CH:4]([PH:8](=[O:12])OCC)[O:5][CH2:6][CH3:7])[CH3:2].[CH2:13]([Mg]Cl)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.C(=O)([O-])[O-].[K+].[K+]>C(OCC)C.O>[CH2:13]([PH:8](=[O:12])[CH:4]([O:3][CH2:1][CH3:2])[O:5][CH2:6][CH3:7])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

참가 물질

6

반응물 3

HCID 11430Potassium CarbonateHCID 178418336HCID 178418336, 화합물HCID 178472284HCID 178472284, 화합물

생성물 1

HCID 178472280HCID 178472280, 화합물

시약·촉매·용매 2

HCID 962Water용매HCID 3283Diethyl Ether용매

실험 절차

By a procedure analogous to that of Example 1, but using 1.96 g of ethyl diethoxymethylphosphinate and 20 ml of a molar solution of benzylmagnesium chloride in diethyl ether and adding 4.14 g of potassium carbonate in 5 ml of water to precipitate inorganic salts, benzyl (diethoxymethyl) phosphine oxide is obtained as a colourless oil.

후처리

  1. customto precipitate inorganic salts

출처 및 근거

ORD 기록
ord-fd52caa51c214f8ea9275e21ac0c4034
출처 데이터셋
uspto-grants-1994_03
특허 번호
US05298663

연결된 노트

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